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First, you did spell nuptial correctly. Good job!

Now, I wouldn't suggest putting newly mated queens in a plaster nest at first, as most species prefer a confined area to raise their brood. I say use test tubes, then transfer the ants to the plaster nest after the first 5 workers eclose, and feed them right away.

I suggest hydrostone as opposed to plaster of paris. It's stronger and more resistant to crumbling when exposed to moisture. And the ants can breathe very well in plaster because it is quite porous.

I don't know any specific details for the species you want, but flights usually take place either at sunrise or sunset, after a medium-heavy rainfall on a nice warm day anywhere from May to August-September.

Getting ants to mate in captivity is quite difficult, even using your greenhouse idea. They prefer being out in the open. It's quite easy to spot newly mated queens after a flight because they are looking for cover, and may have removed their wings.

I hope some of this helps.

Edit: And the term for multi-queen species is "polygynous" I believe. And single-queen species are called "monogynous."